~ 4000 BCE - Papyrus dated as far back as the 4 millennium BCE

Papyrus was first manufactured in Egypt as far back as the fourth millennium BCE. The earliest archaeological evidence of papyrus was excavated in 2012 and 2013 at Wadi al-Jarf, an ancient Egyptian harbor located on the Red Sea coast. These documents, the Diary of Merer, date from c. 2560–2550 BCE (end of the reign of Khufu).[4] The papyrus rolls describe the last years of building the Great Pyramid of Giza.[6] In the first centuries BCE and CE, papyrus scrolls gained a rival as a writing surface in the form of parchment, which was prepared from animal skins.Sheets of parchment were folded to form quires from which book-form codices were fashioned. Early Christian writers soon adopted the codex form, and in the Græco-Roman world, it became common to cut sheets from papyrus rolls to form codices.